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The Analyst Volume 14: (English)

The Analyst Volume 14: (English)

          
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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1889 Excerpt: ...and when dry allowed to cool and finally weighed. Fatty acid (insoluble) in 2 5 grammes 2-2487 2 2502 2-2458 x 40 = Per Cent 89 9480 90-0082 89-8320 When the percentage of insoluble fatty acids have been ascertained, add sufficient standard alkali to the flask, heat gently when saponification rapidly takes place, then wash the soap solution thoroughly into a basin and titrate again with standard acid and estimate the amount of alkali now consumed by the insoluble fatty acids. Thus--A. W. Y. iFo Taken 20 00 c.c. 20-00 c.c. 20-00 c.c. Acid required 11-87 11-74 11-94 Consumed.... 8-13 8-26 8-06 Then Kss Consumed by insoluble fatty acids 8-13 8-26 8-06 Consumed by 2-5 grammes butter 10-22 c.c 10-04 c.c. 10-24 c.c. Kso required by soluble fatty acid of 2-5 grammes 2-09 1-78 2-18 The percentage of soluble fatty acid (as butyric) by Reichert-Wollny's process is: --4-37 4-44 4-68 The amount of soluble acids found in the above three samples of butter calculated as butyric acid: --7-35 6-26 7-67 Deduct that found by distillation 4-37 4-44 4-68 2-98 1-82 2-99 Working in the manner above described, we get an accurate estimation of the amount of the total soluble fatty acids contained in a sample of fat, and it is, therefore, an infinitely superior process to Reichert's, for by the latter only a proportion of the soluble acids are obtained, and that merely of the volatile acids; besides, the Keichert-Wollny method only furnishes comparative results when rigidly performed in the same manner, a process which ought not to be tolerated when there is another method which gives with absolute accuracy the total amount of soluble fatty acids, ileichert's process certainly allows the operator to make a very rough estimation of the volatile acids, but it does not give him any insig...


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Product Details
  • ISBN-13: 9781236049650
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 126
  • Series Title: English
  • Weight: 240 gr
  • ISBN-10: 1236049659
  • Publisher Date: 01 May 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Spine Width: 7 mm
  • Width: 189 mm


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