Home > Qualitative Chemical Analysis, Organic and Inorganic: (English)
Qualitative Chemical Analysis, Organic and Inorganic: (English)

Qualitative Chemical Analysis, Organic and Inorganic: (English)

          
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About the Book

This historic book may have numerous typos and missing text. Purchasers can usually download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1910 edition. Excerpt: ...the solution as sodium chromate, sodium antimonate, etc. II. (a.) Insoluble silicates. Supposing it is required to analyse glass, porcelain, or other silicates, they can be brought into a condition for analysis by fusion as already described for the sulphates. Sodium silicate, which is soluble in water, is produced; aluminium would also be converted into the soluble sodium aluminate, whereas iron would remain as a residue when the melt was treated with water. The solution, after acidifying with hydrochloric acid, is evaporated to dryness, when the silica is obtained as insoluble Si02, and on extracting with dilute hydrochloric acid is left behind. (b.) Or the silicate may be heated with hydrofluoric acid, t Nickel may also be used, but in this case usually a small amount of nickel will be found in the fuse. Silver is really the most satisfactory. when the silica is converted into silicon tetrafluoride, which is driven off on heating. III. Insoluble tin compounds, such as native tin stone, are best converted into the soluble condition by fusion with sulphur and sodium carbonate. Mix the dried substance with five or six times its weight of a mixture of equal parts of sulphur and dry sodium carbonate. Place in a crucible and put on the lid; now heat over a small Bunsen flame until all the sulphur has burned off. On cooling, treat the fuse with hot water and filter. The insoluble portion may consist of the sulphides of other metals which do not form thio-compounds. The tin is obtained in the form of sodium thio-stannate--2SnO2 + 2Na2C03 + 9S = 2Na2SnS3 + 3S02 + 2C02 Insoluble halogen salts, which can only be silver salts, may be decomposed by bringing them in contact with zinc in presence of dilute sulphuric acid. Zn + 2AgCl = 2Ag+ ZnCl, The...


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Product Details
  • ISBN-13: 9781152585515
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 94
  • Series Title: English
  • Weight: 181 gr
  • ISBN-10: 1152585517
  • Publisher Date: 01 Oct 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Spine Width: 5 mm
  • Width: 189 mm


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