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Home > History and Archaeology > History > Technical Methods of Chemical Analysis Volume 2, PT. 1: (English)
Technical Methods of Chemical Analysis Volume 2, PT. 1: (English)

Technical Methods of Chemical Analysis Volume 2, PT. 1: (English)

          
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About the Book

This historic book may have numerous typos and missing text. Purchasers can download a free scanned copy of the original book (without typos) from the publisher. Not indexed. Not illustrated. 1911 Excerpt: ...flask, and to add approximately the same amount of iron (as ferric chloride solution), to dilute, add excess of ammonia and ammonium carbonate, make up to 500 c.c., etc. The amount of zinc retained by the ferric hydroxide precipitate is then approximately the same in both cases. This method is quicker than the above. The excess of ammonia in the solutions to be titrated must be slight; it is usual to allow solutions withdrawn by the pipette to stand uncovered overnight. The sodium sulphide solution is prepared from a cold, saturated solution of pure crystallised sodium sulphide by diluting with ten to twenty times the volume of distilled water and connecting up from a large stock bottle permanently with a burette. The best indicator for the end-point is "Polka paper," a paper sized and covered with white lead; it is prepared for the use of zinc metallurgical laboratories. The titration is carried out in strong beakers (battery glasses) and the solution stirred with a glass rod, which serves for the removal of drops of liquid from time to time which are allowed to drop on to the test paper. A modification of the method of titration consists in adding a flake of freshly precipitated ferric hydroxide to the solution contained in a flask, keeping the solution rapidly rotating during the addition of the sodium sulphide solution and continuing until the flake is blackened. The flask is frequently held over a plateglass mirror to facilitate the observation of the flakes. The method is sufficiently accurate for all technical purposes. (I?) Gallettfs Potassium Ferrocyanide Metltod, modified by Fahlberg,1 v. Schulz, Low,2 and others, consists in precipitating the zinc by means of a solution of potassium ferrocyanide in a solution warmed to 60 to 80, acidifi...


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Product Details
  • ISBN-13: 9781130195460
  • Publisher: Rarebooksclub.com
  • Publisher Imprint: Rarebooksclub.com
  • Height: 246 mm
  • No of Pages: 268
  • Series Title: English
  • Weight: 485 gr
  • ISBN-10: 1130195465
  • Publisher Date: 01 Mar 2012
  • Binding: Paperback
  • Language: English
  • Returnable: N
  • Spine Width: 14 mm
  • Width: 189 mm

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